ARCHIVE

Aviation materials and technologies №1, 2015

Contents

  • E.N. Kablov

    Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»

    3-33
  • E.N. Kablov, O.G. Ospennikova, N.V. Petrushin

    New single crystal heat-resistant intermetallic γ’-based alloy for GTE blades

    34-40
  • R.M. Nazarkin

    X-ray diffraction techniques for precise determination of lattice constants in Ni-based superalloys: a brief review

    41-48
  • D.V. Zaitsev, I.A. Treninkov, A.A. Alekseev

    Ultrafine lamellar precipitation in Ni-based superalloys

    49-55
  • E.A. Davydova, E.B. Chabina, N.S. Moiseeva

    An influence of gadolinium and the method of its introduction on the structure and phase composition of sintered hard magnetic materials of Pr-Dy-Fe-Co-B series

    56-59
  • O.B. Timofeyeva, V.G. Kolodochkina, N.F. Shvanova, A.V. Neiman

    The microstructure analysis of niobium-based high-temperature natural composite material reinforced with niobium silicide intermetallics

    60-64
  • O.Yu. Sorokoin

    On the issue of the mechanism of interaction between carbon materials and Si melt (review)

    65-70
  • M.Yu. Fedotov

    Concepts of creation and trends of smart materials development (review)

    71-80
  • V.V. Murashov, K.S. Mishurov

    Assessment of strength characteristics of carbon fiber reinforced plastics by acoustic method

    81-85
  • S.A. Karimova, A.E. Kutyrev, M.A. Fomina, D.V. Chesnokov

    Modeling of process of influence of aggressive components of the industrial atmosphere on metal materials in the salt spray chamber

    86-94
Содержание номера
1.

DOI: 10.18577/2071-9140-2015-0-1-3-33

UDC: 629.7:620.22

Pages:: 3-33

E.N. Kablov1

[1] Federal state unitary enterprise «All-Russian Scientific-Research Institute of Aviation Materials» of National Research Center «Kurchatov Institute»

Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»

The main results of innovative activities of the Institute from 2011 to 2014 are presented. Special attention is paid to the scientific and technical achievements in the field of developments of materials and technologies of new generation due to a creative cooperation with academic institutes, state scientific centers, national research universities, leading higher education institutions, state corporations and integrated enterprises, scientific organizations and industrial enterprises of 15 regions of Russia. Examples of realization of materials science developments and recommendations on their application for creation of advanced innovative concepts defined in «Strategic directions of the development of materials and technologies of their processing for the period until 2030» are given.

Keywords: high heat-resistan, aluminum, titanium and magnesium alloys, binding and polymer composite materials, organic plastics, fiberglass, carbon fiber reinforced plastics, high-temperature heat-protective ceramic materials, weldable high-strength corrosion-resistant alloys and steels, energy-saving, resource saving and additive technologies, complex corrosion protection, strengthening, wear-resistant protective and heat-insulting coatings, climatic tests, methods of materials qualification and non-destructive testing

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    100. Mekalina I.V., Bogatov V.A., Trigub T.S., Sentjurin E.G. Aviacionnye organicheskie stekla [Aviation organic glass] //Trudy VIAM. 2013. №11. St. 04 (viam-works.ru). 

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    105. Kisljakov P.P., Hohlov Ju.A., Krynin A.G., Kondrashov S.V. Poluchenie i primenenie polimernoj plenki s prozrachnym jelektroprovodjashhim pokrytiem na osnove oksida indija, legirovannogo olovom [Preparation and use of a polymer film coated with a transparent conductive indium oxide doped with tin] //Trudy VIAM. 2013. №11. St. 06 (viam-works.ru).

    106. Hohlov Ju.A., Krynin A.G., Bogatov V.A., Kisljakov P.P. Opticheskie konstanty tonkih plenok oksida indija, legirovannogo olovom, osazhdennyh na polijetilentereftalatnuju plenku metodom reaktivnogo magnetronnogo raspylenija (blizhnjaja infrakrasnaja oblast' spektra) [The optical constants of thin films of indium oxide doped with tin deposited on PET film by reactive magnetron sputtering (NIR)] //Aviacionnye materialy i tehnologii. 2013. №1. S. 24–28. 

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    111. Demin S.A., Gubenkova O.A., Karimova S.A., Vinogradov S.S. Termostojkoe kompozicionnoe pokrytie na osnove fosfatov dlja zashhity vysokoprochnyh stalej ot korrozii [Heat resistant composite phosphate coatings to protect against corrosion high strength steels] //Stal'. 2013. №6. S. 77–79.

    112. Kozlov I.A., Karimova S.A. Korrozija magnievyh splavov i sovremennye metody ih zashhity [Corrosion of Magnesium Alloys and modern methods of protection] //Aviacionnye materialy i tehnologii. 2014. №2. S. 15–20.

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    116. Platonov M.M., Nesterova T.A., Nazarov I.A., Bejder Je.Ja. Pozharobezopasnyj material na tekstil'noj osnove s poliuretanovym pokrytiem dlja naduvnoj obolochki spasatel'nogo trapa [Fireproof material textile-based polyurethane-coated shell for inflatable rescue ladder] //Aviacionnye materialy i tehnologii. 2013. №2. S. 50–54.

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    121. Kondrashov Je.K., Kozlova A.A., Malova N.E. Issledovanie kinetiki otverzhdenija ftorpoliuretanovyh jemalej alifaticheskimi poliizocianatami razlichnyh tipov The study of the kinetics of curing ftorpoliuretanovyh enamels aliphatic polyisocyanates different types [The study of the kinetics of curing ftorpoliuretanovyh enamels aliphatic polyisocyanates different types] //Aviacionnye materialy i tehnologii. 2013. №1. S. 48–49. 

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    123. Kuznecova V.A., Semenova L.V., Kondrashov Je.K., Lebedeva T.A. Lakokrasochnye materialy s ponizhennym soderzhaniem vrednyh i toksichnyh komponentov dlja okraski agregatov i konstrukcij iz PKM [Coating materials with a low content of harmful and toxic components for dyeing units and structures of the PCM] //Trudy VIAM. 2013. №8. St. 05 (viam-works.ru).

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    125. Solncev S.S., Rozenenkova V.A., Mironova N.A., Gavrilov S.V. Vysokotemperaturnye pokrytija SiC–Si3N4–SiO2 dlja voloknistyh metallicheskih uplotnitel'nyh materialov [High temperature coating SiC–Si3N4–SiO2 for fibrous metal sealing materials] //Steklo i keramika. 2011. №6. S. 27–31.

    126. Kablov E.N., Solncev S.S., Rozenenkova V.A., Mironova N.A. Kompozicionnye steklometallicheskie pokrytija dlja zashhity berillija pri vysokih temperaturah [Glass-metal composite coating to protect the beryllium at high temperatures] //Steklo i keramika. 2012. №4. S. 12–16.

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    128. Kablov E.N., Kirillov V.N., Zhirnov A.D., Starcev O.V. Vapirov Ju.M. Centry dlja klimaticheskih ispytanij aviacionnyh PKM [The Centers for climatic test aircraft PCM] //Aviacionnaja promyshlennost'. 2009. №4. C. 36–46.

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    153. Gorbovec M.A., Bazyleva O.A., Beljaev M.S., Hodinev I.A. Malociklovaja ustalost' monokristallicheskogo intermetallidnogo splava tipa VKNA v uslovijah «zhestkogo» nagruzhenija [Low cycle fatigue monocrystalline intermetallic alloy type VKNA in a «hard» loading] //Metallurg. 2014. №8. S. 111–114.

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    156. Orlov M.R., Naprienko S.A., Lavrov A.V. Fraktograficheskij analiz jekspluatacionnogo razrushenija diska kompressora vysokogo davlenija iz splava VT18U [Fractographic analysis of operational failure drive the high pressure compressor of an alloy VT18U] //Titan. 2014. №2. S. 16–21.

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    162. Alekseev A.V., Jakimovich P.V. Opredelenie mysh'jaka i selena v zharoprochnyh nikelevyh splavah metodom ISP-MS s gidridnoj generaciej parov [Determination of arsenic and selenium in the heat-resistant nickel alloys by ICP-MS with a hydride vapor generation] //Trudy VIAM. 2014. №11. St. 09 (viam-works.ru).

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2.

DOI: 10.18577/2071-9140-2015-0-1-34-40

UDC: 669.017.165:669.018.44

Pages:: 34-40

E.N. Kablov1, O.G. Ospennikova1, N.V. Petrushin1

[1] Federal state unitary enterprise «All-Russian Scientific-Research Institute of Aviation Materials» of National Research Center «Kurchatov Institute»

New single crystal heat-resistant intermetallic γ’-based alloy for GTE blades

Development of a new single crystal heat-resistant intermetallic Ni-Al-Cr-Mo-W-Ta alloy (VIN3) performed via CAD is described in the paper. Single crystal alloy VIN3 with [001] orientation and low density (8.25 g/сm3) has high phase stability. Its short-time strength characteristics at 900-1200°C are substantially (by 20-60%) higher than those of heat-resistant intermetallic alloys VKNA-1V with [111] orientation and VKNA-25 (VIN1) with [001] orientation; the alloy is superior to heat-resistant intermetallic VKNA-25 alloy (VIN1) with [001] orientation in long-term strength at 1200°С. VIN3 alloy with [001] orientation can be recommended for production of GTE rotor blades and vanes operating at temperatures up to 1200°С and up to 1250°С within a short space of time.

Keywords: heat-resistant intermetallic alloy, crystallographic orientation, phase stability, single crystal structure, computer-aided design, GTE blades

Reference List

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    19. Ni3Al-based intermetallic alloys having improved strength above 850°C: pat. №6106640 US; pabl. 22.08.200

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DOI: 10.18577/2071-9140-2015-0-1-41-48

UDC: 620.179.1

Pages:: 41-48

R.M. Nazarkin1

[1] ALL-RUSSIAN SCIENTIFIC RESEARCH INSTITUTE OF AVIATION MATERIALS, admin@viam.ru

X-ray diffraction techniques for precise determination of lattice constants in Ni-based superalloys: a brief review

The most widely used techniques of X-ray diffraction analysis of nickel-based superalloys described in Russian and foreign references are presented in this paper. In addition, fields of application and capabilities of modern techniques for precise determination of crystal lattice constants of γ/γʹ-phases in Ni-based superalloys are demonstrated. An influence of internal elastic stresses in a crystal on X-ray diffraction reflexes splitting and results of X-ray diffraction analysis are discussed. Schemes of X-ray diffraction reflexes splitting and models of their interpretation for determination of crystal lattice constants and misfit of γ/γʹ-phases in Ni-based superalloys are shown in the review.

Keywords: misfit, Ni-based superalloys, single crystals, lattice constant

Reference List

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DOI:  10.18577/2071-9140-2015-0-1-49-55

UDC: 669.245.018.44

Pages:: 49-55

D.V. Zaitsev1, I.A. Treninkov2, A.A. Alekseev3

[1] Federal state unitary enterprise «All-Russian Scientific-Research Institute of Aviation Materials» of National Research Center «Kurchatov Institute»
[2] Federal State Unitary Enterprise «All-Russian Scientific Research Institute of Aviation Materials»
[3] Federal state unitary enterprise «All-Russian Scientific-Research Institute of Aviation Materials» of National Research Center «Kurchatov Institute» State research center of the Russian Federation, admin@viam.ru

Ultrafine lamellar precipitation in Ni-based superalloys

Clusters of lamellar precipitates of topological close packed phase (T-phase) in heat-resistant single crystal Ni-based alloy VZHM6 were investigated using X-Ray structure microanalysis (XRSMA) and TEM methods. Crystal system of T-phase lattice was assessed as a triclinic structure. Qualitative assessment of the elemental composition of the obtained particles was performed. An interaction of T-phase width γ-, γ'-phase structure was studied. It was shown that formation of T-phase plate structure depends on periodicity of the initial structure retaining during creep process and influencing formation of the raft structure. An interaction of T-phase plates with dislocation structure in VZHM6 alloy after long-term strength testing was studied using TEM. It is shown that T-phase plates contribute to an additional hardening of the alloy during deformation.

Keywords: Ni-based superalloys, phase transformation, crystal lattice, TEM, X-Ray structure analysis

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DOI: 10.18577/2071-9140-2015-0-1-56-59

UDC: 669.85:620.179

Pages:: 56-59

E.A. Davydova1, E.B. Chabina2, N.S. Moiseeva1

[1] Federal state unitary enterprise «All-Russian Scientific-Research Institute of Aviation Materials» of National Research Center «Kurchatov Institute» State research center of the Russian Federation, admin@viam.ru
[2] Federal state unitary enterprise «All-Russian Scientific-Research Institute of Aviation Materials» of National Research Center «Kurchatov Institute»

An influence of gadolinium and the method of its introduction on the structure and phase composition of sintered hard magnetic materials of Pr-Dy-Fe-Co-B series

Structure, phase composition and nature of the alloying elements distribution in the structure of sintered hard magnetic material of Pr-Dy-Fe-Co-B series in case of introduction of gadolinium at the stages of milling and sintering were investigated. Local chemical composition and stoichiometry of the detected phases were defined.

Keywords: X-ray spectrum microanalysis, X-ray structure analysis, microstructure, sintered hard magnetic materials

Reference List

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    2. Horev A.I., Nochovnaja N.A., Jakovlev A.L. Mikrolegirovanie redkozemel'nymi metallami titanovyh splavov [Microalloying rare earth metals titanium alloys] //Aviacionnye materialy i tehnologii. 2012. №S. S. 206–212.

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    4. Mel'nikov S.A., Piskorskij V.P., Beljaev I.V., Valeev R.A., Verklov M.M., Ivanov S.I., Ospennikova O.G., Parshin A.P. Temperaturnye zavisimosti magnitnyh svojstv spechennyh splavov Nd–Fe–B, legirovannyh splavami RZM s perehodnymi metallami [The temperature dependence of the magnetic properties of the sintered alloy Nd–Fe–B, RE alloys doped with transition metals] //Perspektivnye materialy. 2011. Spec. vyp. (11). S. 201–207.

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    7. Piskorskij V.P., Burhanov G.S., Ospennikova O.G., Valeev R.A., Tereshina I.S., Davydova E.A. Raschet temperaturnogo kojefficienta indukcii nanostrukturirovannyh magnitotverdyh materialov Pr–Dy–Gd–Fe–Co–B metodom molekuljarnogo polja [The calculation of the temperature coefficient of induction of nanostructured magnetic materials Pr–Dy–Gd–Fe–Co–B by molecular field] //Metally. 2010. №1. S. 64–67.

    8. Kablov E.N., Ospennikova O.G., Vershkov A.V. Redkie metally i redkozemel'nye jelementy – materialy sovremennyh i budushhih vysokih tehnologij [Rare metals and rare earth elements - materials of current and future high-tech] //Trudy VIAM. 2013. №2. St. 01 (viam-works.ru).

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    13. Petrakov A.F., Piskorskij V.P., Burhanov G.S., Repina M.V., Ivanov S.I. Osobennosti spekanija magnitov Nd(Pr)–Dy–Fe–Co–B c vysokim soderzhaniem So [Features sintering magnets Nd(Pr)–Dy–Fe–Co–B c high content of Co] //MiTOM. 2012. №7. S. 3–9.

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    16. Cook B.A., Harringa J.L., Laabs F.C., Dennis K.W., Russell A.M., McCallum R.W. Diffusion of Fe, Co, Nd, and Dy in R2(Fe1-xCox)14B, where R=Nd or Dy //Journal of Magnetism and Magnetic Materials. 2001. V. 233. P. L136–L141.

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DOI: 10.18577/2071-9140-2015-0-1-60-64

UDC: 669.293:620.186

Pages:: 60-64

O.B. Timofeyeva1, V.G. Kolodochkina2, N.F. Shvanova1, A.V. Neiman1

[1] Federal state unitary enterprise «All-Russian Scientific-Research Institute of Aviation Materials» of National Research Center «Kurchatov Institute» State research center of the Russian Federation, admin@viam.ru
[2] Federal state unitary enterprise «All-Russian Scientific-Research Institute of Aviation Materials» of National Research Center «Kurchatov Institute»

The microstructure analysis of niobium-based high-temperature natural composite material reinforced with niobium silicide intermetallics

The microstructure of niobium-based high-temperature natural composite material reinforced with niobium silicide intermetallics was investigated as-cast and after directional solidification by scanning electron microscopy.

Keywords: composite material, directional solidification, scanning electron microscopy, microstructure, niobium silicide intermetallics

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    10. Sheftel' E.N., Bannyh O.A. Fiziko-himicheskie i strukturnye podhody k sozdaniju kon-strukcionnyh splavov na osnove niobija [Physico-chemical and structural approaches to the creation of structural alloys based on niobium] //Tehnologija metallov. 2009. №5. S. 42–49; №6. S. 42–49.

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    13. Gerasimov V.V., Demonis I.M. Formirovanie kompozicionnoj struktury v jevtekticheskih splavah pri poluchenii lopatok GTD [Formation of composite structures in eutectic alloys in the preparation of gas turbine engine blades] //Trudy VIAM. 2013. №6. St. 01 (viam-works.ru). 

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    16. Turchenkov V.A., Baranov D.E., Gagarin M.V., Shishkin M.D. Metodicheskij podhod k provedeniju jekspertizy materialov [Methodical approach to the examination of materials] //Aviacionnye materialy i tehnologii. 2012. №1. S. 47–53.

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    19. Mak-Ivili A.Dzh. Rastrovyj jelektronnyj mikroskop [Scanning electron microscope] /V sb. Analiz avarijnyh razrushenij. M.: Tehnosfera. 2010. S. 120–124.

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DOI: 10.18577/2071-9140-2015-0-1-65-70

UDC: 666.7

Pages:: 65-70

O.Yu. Sorokoin1

[1] Federal state unitary enterprise «All-Russian Scientific-Research Institute of Aviation Materials» of National Research Center «Kurchatov Institute» State research center of the Russian Federation, admin@viam.ru

On the issue of the mechanism of interaction between carbon materials and Si melt (review)

The state of the art of high-temperature materials with working temperatures higher than 1650°С was shown. However, C-SiC materials are still of interest in manufacturing of large-sized parts, for example, a nose cone produced by liquid silicon infiltration for an experimental shuttle orbiter. With the purpose to control phase composition of C-SiC material and to avoid erosion of carbon fibers when being siliconized, it is crucial to understand the mechanism of interaction between carbon material and Si. Some possible mechanisms of carbide formation are highlighted, i.e. diffusion-based and solution-precipitation ones. It was shown that there is no full agreement concerning the above mechanism up to now. Nevertheless, the obtained experimental data indicate the multistage nature of the mechanism of siliconization as well as a strong influence of structural peculiarities of carbon materials on the siliconization process. Further studies with the use of up-to-date investigation methods are necessary to define more precisely the siliconization mechanism.

Keywords: carbon fiber, mechanism of SiC formation, composite, silicon

Reference List

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DOI: 10.18577/2071-9140-2015-0-1-71-80

UDC: 620.1:681.785.5

Pages:: 71-80

M.Yu. Fedotov1

[1] Federal state unitary enterprise «All-Russian Scientific-Research Institute of Aviation Materials» of National Research Center «Kurchatov Institute» State research center of the Russian Federation, admin@viam.ru

Concepts of creation and trends of smart materials development (review)

Concepts of creation of smart materials are considered. The domestic and world experience of creation of smart polymer composite materials with fiber-optic systems of built-in control of stress-strain state is summarized.

Keywords: smart material, smart polymer composite material, deformation, stress-strain state, sensor, fiber-optic sensor

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9.

DOI: 10.18577/2071-9140-2015-0-1-81-85

UDC: 620.179:678.747.2

Pages:: 81-85

V.V. Murashov1, K.S. Mishurov1

[1] Federal state unitary enterprise «All-Russian Scientific-Research Institute of Aviation Materials» of National Research Center «Kurchatov Institute»

Assessment of strength characteristics of carbon fiber reinforced plastics by acoustic method

The article dwells upon a dependence of mechanical characteristics of polymer composite material (shear strength and compression strength) and acoustic characteristics (speed and attenuation of ultrasonic vibrations at their distribution in material) of carbon fiber reinforced plastic (CFRP) specimens. It is shown that both strength and acoustic characteristics of material depend on ratio of basic components of plastic and on material porosity, i.e. CFRP micro- and macrostructure. It is also shown that there is a quite close correlation between mechanical and acoustic characteristics, which was used for nondestructive testing of CFRP strength.

Keywords: polymer composite material, carbon fiber reinforced plastics (CFRP), strength characteristics, shear strength, compression strength, acoustic characteristics, porosity of material, correlation, methods of non-destructive testing

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10.

DOI: 10.18577/2071-9140-2015-0-1-86-94

UDC: 620.165.79

Pages:: 86-94

S.A. Karimova1, A.E. Kutyrev2, M.A. Fomina2, D.V. Chesnokov2

[1] Federal state unitary enterprise «All-Russian Scientific-Research Institute of Aviation Materials» of National Research Center «Kurchatov Institute» State research center of the Russian Federation, admin@viam.ru
[2] Federal state unitary enterprise «All-Russian Scientific-Research Institute of Aviation Materials» of National Research Center «Kurchatov Institute»

Modeling of process of influence of aggressive components of the industrial atmosphere on metal materials in the salt spray chamber

Modeling of processes of influence of aggressive components of the industrial atmosphere on metal materials in the salt spray chamber (SSC) is carried out. It is made for development of methods of corrosion tests of materials for assessment of operability of devices in all weather conditions of operation. Two approaches for development of model are offered dissolution and dissosiation of aggressive components of the atmosphere in phase film of moisture on metallic surface; joint adsorption of aggressive components of the atmosphere and vapors of water on metallic surface. For development of testing method preferably have to use phase film model. Tests of systems of the materials used in instrument making in SSC with spraying of solution of sulfite sodium have been carried out. It is established that error-free running time of these systems of materials depends on logarithm of concentration of sprayed solution. It gives the chance of use of provisions state standard specifications R 51372-99 for development of test method for the purpose of determination of operability of devices and the equipment.

Keywords: accelerated corrosion tests, test methods, operating conditions, working capacity assessment, modeling of processes

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